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SCION 456-GC Specification Sheet

SCION 456-GC Specification Sheet

Dimensions and Weights

Size*: Height: 57 cm (22.5 in.) Width: 66 cm (26.0 in.) Depth: 56 cm (22.0 in.) Weight*: 43 kg (95 lb)

* Typical values

Environmental Conditions

Operating temperatures: 10 °C to 40 °C.
Operating humidity (relative): 5 % to 95 %
Line voltage requirements:, 120 V, 230 V (±10 % nominal)

Column Oven

Dimensions: 28 cm (w) x 20 cm (d) x 28 cm (h) Temperature range:

Ambient +4 °C to 450 °C Liquid N2: -100 °C to 450 °C Liquid CO2: -60 °C to 450 °C

Temperature program ramps/holds: 24/25
Maximum temperature ramp rate: 150°C/min for all voltages and 180 °C/min with oven insert accessory

Cool down rate: 400 °C to 50 °C in 4.5 minutes
Temperature set-point resolution: 0.1 °C
Ambient temperature reject <0.01°C change in oven for 1°C change in ambient temp
Retention time Repeatability <0.008% or < 0.0008 min, based on Pentadecane under temperature program conditions
Area repeatability < 1% RSD

General Specifications

Up to 9 EFC modules total, injector, detector and auxiliary Optional backflush
GC Control:

External events (digital output): · 8 standard
· 8 optional, total 16

Max number of timed events: 16 Heated zones:

· Standard 5
· 4 optional, 9 total

Two power outlets 24V (1A max. each)

Methods:
Maximum stored internal methods: 50 (max. 30 alphanumeric characters)

For research use only. Not for use in diagnostic procedures. Scion Instruments

Temperature Range (°C)

456-GC Rates (°C/min)

50 -70

150

70 – 115

95

115 – 175

70

175 – 300

45

300 – 450

30

www.scionInstruments.com

3500 West Warren Avenue Fremont CA 94538, USA

Logging:
Run log file (stored with the chromatogram when using CompassCDS) Error log file

Local Display:
TFT full color screen
WVGA resolution (800 x 480) Size 23 cm (9″)

Local Control: Touch screen Hard keys

Languages:
English, German, French, Spanish, Italian, Portuguese, Cyrillic, Kanji, Chinese (standard and traditional), Thai, Korean and Dutch.

Local automation: Method lines: 25 Modes:

· Infinite looping
· Dual and duplicate injection

Communication

Ethernet: Protocol: TCP/IP
Data rate: 100 Mbps
Control: GC control and method parameters Analog output (optional):

Number of channels: 3
Time programmable steps: 30
Output software selectable (set individual):

· 0-1 V (default) · 0-10 V

Synchronization signals with other devices and data systems: Ready in and out
Start in and out

Data Handling and System Control: CompassCDS Chromatography Data System

Certifications

CSA:

  • ·  C22.2 61010-1
  • ·  UL 61010-1IEC: 61010-1 EMC:
    • ·  47 CFR part 15
    • ·  ANSI C63.4
    • ·  EN 61326For research use only. Not for use in diagnostic procedures. www.scionInstruments.com

Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA

Injector Options

Maximum injectors: three, operating concurrently Pneumatics: Electronic Flow Control (EFC), or manual Injector types:

S/SL Split/Splitless injector*
PTV Programmable Temperature Vaporizing* COC Cold On-Column injector*
Flash injector
PWOC Packed/Wide bore On-Column injector

*Including septum purge

S/SL Split/Splitless Injector

Pressure range: 0-150 psi Total flow:

500 mL/min for N2/Ar

1500 mL/min for He/H2
Maximum temperature: 450 °C
Split range: 1-10,000 (column dependent)

Suited for columns:
Wide bore: (0.53 mm)
Narrow bore: (0.05 to 0.32 mm)

COC Cold On-Column Injector

Pressure range: 0-150 psi
Total Flow: 50 mL/min (Type 23 EFC)

Temperature range:
Ambient +10 °C to 450 °C using air cooling -60°Cto450°CusingliquidCO2 cooling -160 °C to 450 °C using liquid N2 cooling

Maximum temperature: 450 °C
Maximum temperature ramp rate: 200 °C/min Temperature ramps/holds: 24/25

Suited for columns:
Wide bore (0.53 mm) Narrow bore (0.32 mm)

PTV Programmable Temperature

Vaporizing Injector Pressure range: 0-150 psi Total flow:

500 mL/min for N2/Ar 1500 ml/min for He/H2

Temperature range:
Ambient + 10 °C to 450 °C using air cooling -160 °C to 450 °C using liquid N2 cooling -60 °C to 450 °C using liquid CO2 cooling

Maximum temperature ramp rate: 200 °C/min Temperature ramps/holds: 24/25
Split range: 1-10,000 (column dependent)

For research use only. Not for use in diagnostic procedures. www.scionInstruments.com

Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA

Operational capabilities:
Large volume injection Temperature ramped splitless Cold on-column

Split and splitless
ChromatoProbe solid sample introduction optional

Suited for columns:
Wide bore (0.53 mm)
Narrow bore (0.05 to 0.32 mm)

Maximum injection volume: 250 μL (LVI mode)

Flash Injector

Pressure range: 0-150 psi Total flow:

50 mL/min (Type 23 EFC)

Maximum temperature: 450 °C Suited for columns:

Wide bore (0.53 mm) Packed (1/8” to 1/4”)

PWOC Packed/Wide-bore On-Column Injector

Pressure range: 0-150 psi Total flow:

50 mL/min (Type 23 EFC) Maximum temperature: 450 °C

Suited for columns:
Wide bore (0.53 mm) Packed (1/8” to 1/4”)

Electronic Flow Control: Injectors (EFC)

Module types: 4 injector-specific modules
Pressure: 0.1 % Full Scale
Resolution pressure set points is 0.001psi
Flow sensor accuracy 2% of measured or 0.2% of full scale Flow sensor repeatability 0.5%

Sample Preconcentration Trap (SPT)

Trace level analysis of volatiles in gases Fully integrated

Temperature range: -60°Cto450°CusingliquidCO2 cooling -185 °C to 450 °C using liquid N2 cooling

Temperature rate:
Ballistic for instant release of adsorbed volatiles

Available traps:
Two lengths
A wide range of standard packings and custom packings

For research use only. Not for use in diagnostic procedures. www.scionInstruments.com

Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA

Quick-Switch Valve Option

Instantly switch between injectors/columns and detectors Configurations: automated or manual, factory or field installed

Detector Options

Maximum detectors: four: operating concurrently (one of which is a Single or Triple Quad MS)
Pneumatics: Electronic Flow Control (DEFC) or manual

Detector types:
FID Flame Ionization Detector
TCD Thermal Conductivity Detector
ECD Electron Capture Detector
NPD (TSD) Nitrogen-Phosphorus Detector
PFPD Pulsed Flame Photometric Detector
PDHID Pulsed Discharge Helium Ionization Detector
MS Mass Spectrometry (see GC/MS brochure and datasheet)

Note: Data Acquisition Rate : 600Hz for all detectors, exception is the PFPD

FID Flame Ionization Detector

Maximum temperature: 450 °C Detectivity: 1.4 pg C/sec
Linear dynamic range: 107

Flame tip type: ceramic (patented) Operational quality:

Flame-out detection Auto re-ignition

TCD Thermal Conductivity Detector

Maximum temperature: 450 °C Detectivity: 300 pg/mL (Butane) Linear dynamic range: 106

Operational quality:
Filament protection Automatic bridge balancing

ECD Electron Capture Detector

Maximum temperature: 450 °C Detectivity: 7 fg/sec Lindane
Linear dynamic range: 104
Radioactive source: 63Ni – 15 mCi (555 Mbq)

NPD (TSD) Nitrogen-Phosphorus Detector

Maximum temperature: 450 °C Detectivity:
N: 100 fg N/sec (Azobenzene)
P: 100 fg P/sec (Malathion)

Linear dynamic range: N: 10 5

P: 10 4
Operational quality: self-aligning bead

For research use only. Not for use in diagnostic procedures. www.scionInstruments.com

Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA

PFPD Pulsed Flame Photometric Detector

Photomultiplier tube: S/P

S/P/N
Maximum temperature: 450 °C

Detectivity:
S: 1 pg S/sec (S/P tube)
P: 100 fg P/sec (S/P tube) N: 20 pg N/sec (S/P/N tube)

Linear dynamic range: S:103

P:104

N:102
Up to 23 elements can be detected

PDHID Pulsed Discharge Helium Ionization Detector

Detectivity: 50 ppb (Methane) Linear dynamic range: 104(Methane) Operational quality:

Gold plated connections Welded column connections

Detectors (DEFC)

Module types: 6 detector-specific modules Accuracy: ± 7 % set point flow
Resolution: 0.1 or 1 mL/min

Automation Options

CP-8410 Auto Injector

Sample capacity: 10 x 2 mL vials 6 x 5 mL vials 5 x 10 mL vials

Large solvent wash vial: 2 x 120 mL* Dual and duplicate mode
Internal standard addition

Modes of operation: Liquid

Ambient headspace*
SPME (Solid Phase MicroExtraction)* Sample heating and cooling*

Pre-programmed modes of injection Syringes:
1 μL, 2 μL, 5 μL, 10 μL, 100 μL, 250 μL for liquid injection SPME

For research use only. Not for use in diagnostic procedures. Scion Instruments

www.scionInstruments.com

3500 West Warren Avenue Fremont CA 94538, USA

CP-8400 AutoSampler

Sample capacity: 100 x 2 mL vials Large solvent wash vial: 2 x 120 mL* Dual and duplicate mode
Internal standard addition

Modes of operation: Liquid

Ambient headspace*
SPME*
Sample heating and cooling*

Pre-programmed modes of injection syringes:
1 μL, 2 μL, 5 μL, 10 μL, 100 μL, 250 μL for liquid injection SPME

* Optional

PAL Combi-xt AutoSampler

Sample trays: two standard and expandable to four Tray types:

98 x 2 mL vials
200 x 1 mL vials
32 x 10 mL/20 mL vials 96-well plates

Dual and duplicate mode Internal standard addition

Modes of operation: Liquid

Heated headspace* SPME*
ITEX*

Sample heating and cooling
Additional optional modules: further sample trays, micro-well plate holders, wash station, SPME fiber bake-out station, dilutor, barcode readers, and flowcell

* Optional

For research use only. Not for use in diagnostic procedures. Scion Instruments

www.scionInstruments.com

3500 West Warren Avenue Fremont CA 94538, USA

SHS-40 Headspace Sampler

Fixed Sample Volume Configuration

SHS-40

Press and Inject Configuration

The

Sample Capacity: 40 x 20ml (10ml vials with adaptors). Fully integrated
Sample path inert
Automated vial queuing system

System Features

Injection Modes

Incubator

Sample Recognition and Detection

Optional Accessories

Fixed Sample Volume Press and Inject

Up to 12 Samples
40-200°C in 1°C increments Integrated Shaker

Automated

Additional Sampling Valve Reactant Gas
Catalytic Converter

Sample Capacity

Up to 40 vials; 20mL
or 10 mL w/adaptor Crimp or Screw Top Vials

Injection Valve

6 Way Electric Actuated 1 mL Sample Loop Heat up to 350°C

Instrument Control

Remote with Compass CDS Stand alone

Carrier Gas Control

Direct from GC

SHS-40

Automated Gas Sampling Valve- Electric actuated 6-way injection valve (VICI) with 1 ml sample loop. This entire module may be separately heated up to 350°C.
Heated incubation oven for 12 samples (40°C – 200°C, in 1°C-steps
Integrated Shaker

Automatic sample detection/recognition Compatible with Crimp and Screw Top Vials Carrier gas controlled direct from the GC AUX gas pre-set internally.

Up to 9 different parameter sets can be stored.
Adaptable to different injectors
Multiple Headspace Extraction mode via single puncture
Flexible transfer line
Option: Sample Transfer Line Kit (direct connection to carrier gas, insertion of transfer line via injector no longer required)
Control: Stand alone or remotely via Compass CDS software
Voltage: 110V or 230V
Dimensions: Width: 29cm (12in) Height: 46cm (18in) Depth: 62cm (25in)
Weight: 21kg (47lb)

For research use only. Not for use in diagnostic procedures. Scion Instruments

www.scionInstruments.com

3500 West Warren Avenue Fremont CA 94538, USA

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