SCION 456-GC Specification Sheet
SCION 456-GC Specification Sheet
Dimensions and Weights
Size*: Height: 57 cm (22.5 in.) Width: 66 cm (26.0 in.) Depth: 56 cm (22.0 in.) Weight*: 43 kg (95 lb)
* Typical values
Environmental Conditions
Operating temperatures: 10 °C to 40 °C.
Operating humidity (relative): 5 % to 95 %
Line voltage requirements:, 120 V, 230 V (±10 % nominal)
Column Oven
Dimensions: 28 cm (w) x 20 cm (d) x 28 cm (h) Temperature range:
Ambient +4 °C to 450 °C Liquid N2: -100 °C to 450 °C Liquid CO2: -60 °C to 450 °C
Temperature program ramps/holds: 24/25
Maximum temperature ramp rate: 150°C/min for all voltages and 180 °C/min with oven insert accessory
Cool down rate: 400 °C to 50 °C in 4.5 minutes
Temperature set-point resolution: 0.1 °C
Ambient temperature reject <0.01°C change in oven for 1°C change in ambient temp
Retention time Repeatability <0.008% or < 0.0008 min, based on Pentadecane under temperature program conditions
Area repeatability < 1% RSD
General Specifications
Up to 9 EFC modules total, injector, detector and auxiliary Optional backflush
GC Control:
External events (digital output): · 8 standard
· 8 optional, total 16
Max number of timed events: 16 Heated zones:
· Standard 5
· 4 optional, 9 total
Two power outlets 24V (1A max. each)
Methods:
Maximum stored internal methods: 50 (max. 30 alphanumeric characters)
For research use only. Not for use in diagnostic procedures. Scion Instruments
Temperature Range (°C) |
456-GC Rates (°C/min) |
50 -70 |
150 |
70 – 115 |
95 |
115 – 175 |
70 |
175 – 300 |
45 |
300 – 450 |
30 |
www.scionInstruments.com
3500 West Warren Avenue Fremont CA 94538, USA
Logging:
Run log file (stored with the chromatogram when using CompassCDS) Error log file
Local Display:
TFT full color screen
WVGA resolution (800 x 480) Size 23 cm (9″)
Local Control: Touch screen Hard keys
Languages:
English, German, French, Spanish, Italian, Portuguese, Cyrillic, Kanji, Chinese (standard and traditional), Thai, Korean and Dutch.
Local automation: Method lines: 25 Modes:
· Infinite looping
· Dual and duplicate injection
Communication
Ethernet: Protocol: TCP/IP
Data rate: 100 Mbps
Control: GC control and method parameters Analog output (optional):
Number of channels: 3
Time programmable steps: 30
Output software selectable (set individual):
· 0-1 V (default) · 0-10 V
Synchronization signals with other devices and data systems: Ready in and out
Start in and out
Data Handling and System Control: CompassCDS Chromatography Data System
Certifications
CSA:
- · C22.2 61010-1
- · UL 61010-1IEC: 61010-1 EMC:
- · 47 CFR part 15
- · ANSI C63.4
- · EN 61326For research use only. Not for use in diagnostic procedures. www.scionInstruments.com
Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA
Injector Options
Maximum injectors: three, operating concurrently Pneumatics: Electronic Flow Control (EFC), or manual Injector types:
S/SL Split/Splitless injector*
PTV Programmable Temperature Vaporizing* COC Cold On-Column injector*
Flash injector
PWOC Packed/Wide bore On-Column injector
*Including septum purge
S/SL Split/Splitless Injector
Pressure range: 0-150 psi Total flow:
500 mL/min for N2/Ar
1500 mL/min for He/H2
Maximum temperature: 450 °C
Split range: 1-10,000 (column dependent)
Suited for columns:
Wide bore: (0.53 mm)
Narrow bore: (0.05 to 0.32 mm)
COC Cold On-Column Injector
Pressure range: 0-150 psi
Total Flow: 50 mL/min (Type 23 EFC)
Temperature range:
Ambient +10 °C to 450 °C using air cooling -60°Cto450°CusingliquidCO2 cooling -160 °C to 450 °C using liquid N2 cooling
Maximum temperature: 450 °C
Maximum temperature ramp rate: 200 °C/min Temperature ramps/holds: 24/25
Suited for columns:
Wide bore (0.53 mm) Narrow bore (0.32 mm)
PTV Programmable Temperature
Vaporizing Injector Pressure range: 0-150 psi Total flow:
500 mL/min for N2/Ar 1500 ml/min for He/H2
Temperature range:
Ambient + 10 °C to 450 °C using air cooling -160 °C to 450 °C using liquid N2 cooling -60 °C to 450 °C using liquid CO2 cooling
Maximum temperature ramp rate: 200 °C/min Temperature ramps/holds: 24/25
Split range: 1-10,000 (column dependent)
For research use only. Not for use in diagnostic procedures. www.scionInstruments.com
Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA
Operational capabilities:
Large volume injection Temperature ramped splitless Cold on-column
Split and splitless
ChromatoProbe solid sample introduction optional
Suited for columns:
Wide bore (0.53 mm)
Narrow bore (0.05 to 0.32 mm)
Maximum injection volume: 250 μL (LVI mode)
Flash Injector
Pressure range: 0-150 psi Total flow:
50 mL/min (Type 23 EFC)
Maximum temperature: 450 °C Suited for columns:
Wide bore (0.53 mm) Packed (1/8” to 1/4”)
PWOC Packed/Wide-bore On-Column Injector
Pressure range: 0-150 psi Total flow:
50 mL/min (Type 23 EFC) Maximum temperature: 450 °C
Suited for columns:
Wide bore (0.53 mm) Packed (1/8” to 1/4”)
Electronic Flow Control: Injectors (EFC)
Module types: 4 injector-specific modules
Pressure: 0.1 % Full Scale
Resolution pressure set points is 0.001psi
Flow sensor accuracy 2% of measured or 0.2% of full scale Flow sensor repeatability 0.5%
Sample Preconcentration Trap (SPT)
Trace level analysis of volatiles in gases Fully integrated
Temperature range: -60°Cto450°CusingliquidCO2 cooling -185 °C to 450 °C using liquid N2 cooling
Temperature rate:
Ballistic for instant release of adsorbed volatiles
Available traps:
Two lengths
A wide range of standard packings and custom packings
For research use only. Not for use in diagnostic procedures. www.scionInstruments.com
Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA
Quick-Switch Valve Option
Instantly switch between injectors/columns and detectors Configurations: automated or manual, factory or field installed
Detector Options
Maximum detectors: four: operating concurrently (one of which is a Single or Triple Quad MS)
Pneumatics: Electronic Flow Control (DEFC) or manual
Detector types:
FID Flame Ionization Detector
TCD Thermal Conductivity Detector
ECD Electron Capture Detector
NPD (TSD) Nitrogen-Phosphorus Detector
PFPD Pulsed Flame Photometric Detector
PDHID Pulsed Discharge Helium Ionization Detector
MS Mass Spectrometry (see GC/MS brochure and datasheet)
Note: Data Acquisition Rate : 600Hz for all detectors, exception is the PFPD
FID Flame Ionization Detector
Maximum temperature: 450 °C Detectivity: 1.4 pg C/sec
Linear dynamic range: 107
Flame tip type: ceramic (patented) Operational quality:
Flame-out detection Auto re-ignition
TCD Thermal Conductivity Detector
Maximum temperature: 450 °C Detectivity: 300 pg/mL (Butane) Linear dynamic range: 106
Operational quality:
Filament protection Automatic bridge balancing
ECD Electron Capture Detector
Maximum temperature: 450 °C Detectivity: 7 fg/sec Lindane
Linear dynamic range: 104
Radioactive source: 63Ni – 15 mCi (555 Mbq)
NPD (TSD) Nitrogen-Phosphorus Detector
Maximum temperature: 450 °C Detectivity:
N: 100 fg N/sec (Azobenzene)
P: 100 fg P/sec (Malathion)
Linear dynamic range: N: 10 5
P: 10 4
Operational quality: self-aligning bead
For research use only. Not for use in diagnostic procedures. www.scionInstruments.com
Scion Instruments
3500 West Warren Avenue Fremont CA 94538, USA
PFPD Pulsed Flame Photometric Detector
Photomultiplier tube: S/P
S/P/N
Maximum temperature: 450 °C
Detectivity:
S: 1 pg S/sec (S/P tube)
P: 100 fg P/sec (S/P tube) N: 20 pg N/sec (S/P/N tube)
Linear dynamic range: S:103
P:104
N:102
Up to 23 elements can be detected
PDHID Pulsed Discharge Helium Ionization Detector
Detectivity: 50 ppb (Methane) Linear dynamic range: 104(Methane) Operational quality:
Gold plated connections Welded column connections
Detectors (DEFC)
Module types: 6 detector-specific modules Accuracy: ± 7 % set point flow
Resolution: 0.1 or 1 mL/min
Automation Options
CP-8410 Auto Injector
Sample capacity: 10 x 2 mL vials 6 x 5 mL vials 5 x 10 mL vials
Large solvent wash vial: 2 x 120 mL* Dual and duplicate mode
Internal standard addition
Modes of operation: Liquid
Ambient headspace*
SPME (Solid Phase MicroExtraction)* Sample heating and cooling*
Pre-programmed modes of injection Syringes:
1 μL, 2 μL, 5 μL, 10 μL, 100 μL, 250 μL for liquid injection SPME
For research use only. Not for use in diagnostic procedures. Scion Instruments
www.scionInstruments.com
3500 West Warren Avenue Fremont CA 94538, USA
CP-8400 AutoSampler
Sample capacity: 100 x 2 mL vials Large solvent wash vial: 2 x 120 mL* Dual and duplicate mode
Internal standard addition
Modes of operation: Liquid
Ambient headspace*
SPME*
Sample heating and cooling*
Pre-programmed modes of injection syringes:
1 μL, 2 μL, 5 μL, 10 μL, 100 μL, 250 μL for liquid injection SPME
* Optional
PAL Combi-xt AutoSampler
Sample trays: two standard and expandable to four Tray types:
98 x 2 mL vials
200 x 1 mL vials
32 x 10 mL/20 mL vials 96-well plates
Dual and duplicate mode Internal standard addition
Modes of operation: Liquid
Heated headspace* SPME*
ITEX*
Sample heating and cooling
Additional optional modules: further sample trays, micro-well plate holders, wash station, SPME fiber bake-out station, dilutor, barcode readers, and flowcell
* Optional
For research use only. Not for use in diagnostic procedures. Scion Instruments
www.scionInstruments.com
3500 West Warren Avenue Fremont CA 94538, USA
SHS-40 Headspace Sampler
Fixed Sample Volume Configuration
SHS-40
Press and Inject Configuration
The
Sample Capacity: 40 x 20ml (10ml vials with adaptors). Fully integrated
Sample path inert
Automated vial queuing system
System Features
Injection Modes
Incubator
Sample Recognition and Detection
Optional Accessories
Fixed Sample Volume Press and Inject
Up to 12 Samples
40-200°C in 1°C increments Integrated Shaker
Automated
Additional Sampling Valve Reactant Gas
Catalytic Converter
Sample Capacity
Up to 40 vials; 20mL
or 10 mL w/adaptor Crimp or Screw Top Vials
Injection Valve
6 Way Electric Actuated 1 mL Sample Loop Heat up to 350°C
Instrument Control
Remote with Compass CDS Stand alone
Carrier Gas Control |
Direct from GC |
SHS-40
Automated Gas Sampling Valve- Electric actuated 6-way injection valve (VICI) with 1 ml sample loop. This entire module may be separately heated up to 350°C.
Heated incubation oven for 12 samples (40°C – 200°C, in 1°C-steps
Integrated Shaker
Automatic sample detection/recognition Compatible with Crimp and Screw Top Vials Carrier gas controlled direct from the GC AUX gas pre-set internally.
Up to 9 different parameter sets can be stored.
Adaptable to different injectors
Multiple Headspace Extraction mode via single puncture
Flexible transfer line
Option: Sample Transfer Line Kit (direct connection to carrier gas, insertion of transfer line via injector no longer required)
Control: Stand alone or remotely via Compass CDS software
Voltage: 110V or 230V
Dimensions: Width: 29cm (12in) Height: 46cm (18in) Depth: 62cm (25in)
Weight: 21kg (47lb)
For research use only. Not for use in diagnostic procedures. Scion Instruments
www.scionInstruments.com
3500 West Warren Avenue Fremont CA 94538, USA
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